Maturation and flavor chemistry; quantitative discrepancy boundaries must travel with any reused claim.
Full article, supplementary document and workbook read. Source-specific paraphrase with analytical limitations, not independent corroboration.
Independent grouping of all supplied cells yields TFA sample counts 8-15 per group, not uniformly 12. TFA group means and standard errors largely match Table S2 to displayed precision. Sulfuric new groups contain 8 observations, not 10; ten-O neutral sugars have two missing dashes. Some sulfuric values differ materially: ten-O glucose G51:G58 mean 47.531 versus published 26.9; ten-P xylose I29:I38 mean 276.979 versus 256.4; ten-R xylose I39:I48 mean 253.073 versus 291.6; ten-O cellulose J49:J58 mean 267.258 versus 298.0. Preserve both reported and recomputed values, do not silently repair the source. This discrepancy is not evidence of misconduct.
Supplementary Tables S2-S4; workbook TFA rows 3-101; Sulfuric acid Method rows 3-58
Supplementary Tables S2-S4; workbook TFA rows 3-101; Sulfuric acid Method rows 3-58
Checked against complete source package. Recomputed means use supplied numeric observations only; missing dashes remain missing. No claims about unprovided raw assays or sensory outcomes.
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Evidence
Paraphrase, not a direct quotation.
Independent grouping of all supplied cells yields TFA sample counts 8-15 per group, not uniformly 12. TFA group means and standard errors largely match Table S2 to displayed precision. Sulfuric new groups contain 8 observations, not 10; ten-O neutral sugars have two missing dashes. Some sulfuric values differ materially: ten-O glucose G51:G58 mean 47.531 versus published 26.9; ten-P xylose I29:I38 mean 276.979 versus 256.4; ten-R xylose I39:I48 mean 253.073 versus 291.6; ten-O cellulose J49:J58 mean 267.258 versus 298.0. Preserve both reported and recomputed values, do not silently repair the source. This discrepancy is not evidence of misconduct.
Location and context
Supplementary Tables S2-S4; workbook TFA rows 3-101; Sulfuric acid Method rows 3-58. Article pages use the PDF page numbering; supplementary tables and workbook cells refer to their own files.
Oak cell-wall sugars during whiskey aging — full article and supplement analysis
Annotation
Use for maturation and flavor chemistry. Preserve the distinction between the authors' reported results and our calculation or methodological assessment. This is not sensory evidence.
Verification checklist
Gollihue et al. 2018 — Workbook sample counts and tables do not fully reconcile